ｻﾝﾌﾟﾙ: '191024 Sample ﾌｧｲﾙ名: 191024 100μg アスコルビン.FD3 分析日時: '09:58:48, 10/24/2019 ｵﾍﾟﾚｰﾀ: 筑波大学 ｺﾒﾝﾄ: ' 光度計 ﾓﾃﾞﾙ: F-7000形分光蛍光光度計 ｼﾘｱﾙ No.: 2357-015 ROM Ver.: 5J14000 06 装置条件 測定ﾓｰﾄﾞ: 3次元 ﾃﾞｰﾀﾓｰﾄﾞ: 蛍光 励起開始波長: 200.0 nm 励起終了波長: 500.0 nm 励起側ｻﾝﾌﾟﾘﾝｸﾞ間隔: 10.0 nm 蛍光開始波長: 200.0 nm 蛍光終了波長: 700.0 nm 蛍光側ｻﾝﾌﾟﾘﾝｸﾞ間隔: 10.0 nm ｽｷｬﾝｽﾋﾟｰﾄﾞ: 30000 nm/min 励起側ｽﾘｯﾄ: 5.0 nm 蛍光側ｽﾘｯﾄ: 5.0 nm ﾎﾄﾏﾙ電圧: 700 V ﾚｽﾎﾟﾝｽ: 自動 ｽﾍﾟｸﾄﾙ補正: On ｼｬｯﾀ制御: On 等高線間隔: 50.000 装置関数 励起側(200〜500nm) ｽﾘｯﾄ：5.0/20.0nm ﾎﾄﾏﾙ電圧：400V 蛍光側(200〜500nm) ｽﾘｯﾄ：5.0/20.0nm ﾎﾄﾏﾙ電圧：250V 蛍光側(500〜900nm) ｽﾘｯﾄ：---/5.0nm ﾎﾄﾏﾙ電圧：400V 励起側(500〜900nm) ｽﾘｯﾄ：5.0/5.0nm ﾎﾄﾏﾙ電圧：350V ﾃﾞｰﾀﾘｽﾄ 200.000 210.000 220.000 230.000 240.000 250.000 260.000 270.000 280.000 290.000 300.000 310.000 320.000 330.000 340.000 350.000 360.000 370.000 380.000 390.000 400.000 410.000 420.000 430.000 440.000 450.000 460.000 470.000 480.000 490.000 500.000 200.0 9999.9 4653 42.44 26.84 15.81 12.21 10.71 13.16 12.38 13.69 13.50 10.58 10.82 10.01 8.888 7.791 7.377 6.437 6.403 6.837 33.68 39.57 5.482 3.903 3.951 2.791 2.709 2.569 2.277 2.198 2.129 210.0 580.4 9999.9 2904 19.98 13.41 10.65 8.184 8.555 8.390 8.397 8.174 8.220 6.336 6.039 5.384 4.891 4.430 4.048 3.670 3.868 4.125 6.607 43.02 47.05 3.197 2.193 2.115 1.526 1.490 1.505 1.627 220.0 75.10 540.7 9999.9 2513 21.09 7.618 7.694 6.348 6.556 7.200 5.724 5.339 4.962 4.602 3.669 3.197 2.909 3.031 2.527 2.595 2.292 2.181 3.306 6.561 56.17 54.23 3.226 1.170 1.143 0.917 1.204 230.0 87.24 100.6 605.1 9999.9 2646 18.01 8.409 7.004 5.305 5.852 5.834 4.638 4.015 3.833 3.579 2.914 2.420 2.302 2.047 1.950 1.898 1.641 1.726 1.371 3.318 10.56 98.65 74.57 3.656 0.996 1.076 240.0 99.52 87.45 97.25 614.3 9999.9 2854 19.68 10.20 7.824 5.619 5.438 4.464 4.389 3.396 3.175 3.095 2.378 2.421 2.215 1.903 1.691 1.383 1.320 1.105 1.082 1.637 4.645 18.41 187.4 137.7 4.693 250.0 158.8 136.3 84.01 91.82 632.0 9999.9 3320 20.68 11.68 8.154 6.597 5.524 4.078 3.514 3.222 3.104 2.633 2.490 2.142 1.933 1.770 1.421 1.274 1.140 1.153 1.176 1.298 1.600 8.201 37.42 338.6 260.0 247.3 149.7 116.9 67.13 88.94 667.4 9999.9 3685 24.79 13.54 9.239 6.201 5.515 4.314 3.490 3.471 2.853 2.608 2.584 1.724 1.712 1.599 1.437 1.437 1.441 1.263 1.127 1.075 1.425 2.542 14.19 270.0 359.2 217.8 122.0 70.45 58.74 91.45 668.1 9999.9 4047 28.93 16.34 10.10 7.206 5.458 4.576 3.985 3.489 3.092 2.743 2.284 2.167 1.703 1.679 1.514 1.372 1.394 1.203 1.162 1.139 1.143 1.802 280.0 388.0 269.7 190.4 82.65 58.39 54.13 88.50 708.1 9999.9 3744 33.16 17.56 10.50 7.783 5.913 4.813 4.074 3.876 3.198 3.047 2.591 2.274 2.021 1.807 1.735 1.546 1.510 1.399 1.346 1.502 1.451 290.0 628.9 412.2 240.7 123.9 68.67 56.19 62.83 97.52 708.8 9999.9 3810 37.05 19.90 11.69 8.213 6.714 5.502 4.705 3.747 3.481 3.102 2.703 2.435 2.322 2.223 1.965 1.883 1.699 1.698 1.729 1.774 300.0 922.3 611.8 351.4 170.0 104.9 74.88 81.20 114.2 135.6 851.6 9999.9 3769 41.98 22.01 14.20 9.902 6.857 5.787 5.193 4.791 4.088 3.664 3.340 2.994 2.900 2.374 2.247 1.905 2.195 2.278 2.332 310.0 1114 699.6 396.1 224.5 113.7 87.12 87.15 105.2 156.3 143.9 849.7 9999.9 3677 44.53 24.71 15.00 10.60 8.030 6.623 5.472 5.002 4.553 4.125 3.917 3.269 3.004 3.087 2.553 2.706 2.764 2.997 320.0 1098 730.4 472.2 247.6 117.5 91.43 88.73 101.1 118.3 166.1 123.0 844.1 9999.9 3813 46.83 26.91 16.35 11.20 8.299 6.963 6.059 5.392 4.607 4.747 4.043 3.452 3.047 2.870 3.066 2.664 2.945 330.0 1211 814.7 529.2 260.7 128.1 84.03 82.60 91.77 105.6 113.3 124.5 102.0 749.1 9999.9 3671 48.72 26.63 17.12 11.89 8.869 7.373 6.126 5.550 5.121 4.845 4.131 3.753 3.019 3.302 2.997 2.951 340.0 1173 851.1 567.8 292.9 155.6 103.0 86.96 87.53 116.0 137.6 99.67 98.14 112.7 685.4 9999.9 3660 48.87 25.42 16.61 11.32 8.191 7.102 6.097 5.534 5.280 4.354 3.986 3.177 3.547 3.444 3.225 350.0 1265 762.7 482.1 290.1 156.1 107.0 87.89 84.08 111.5 143.9 84.66 107.6 90.72 108.3 673.8 9999.9 3647 47.30 24.46 15.74 10.87 8.725 6.965 6.092 5.312 5.034 4.107 3.642 3.409 3.197 3.697 360.0 1247 803.7 457.3 265.9 144.1 105.3 82.32 75.46 102.8 130.8 79.97 75.84 117.8 78.45 91.08 629.8 9999.9 3654 45.04 24.29 15.50 10.95 8.657 7.296 5.778 5.324 4.827 3.858 3.837 3.404 3.319 370.0 1179 844.9 412.2 251.7 133.5 95.75 75.88 72.89 85.76 108.5 75.10 72.89 77.50 106.8 59.26 79.97 596.1 9999.9 3580 43.58 22.88 14.82 11.52 8.125 7.068 5.445 4.845 3.983 4.223 3.620 3.566 380.0 1204 747.7 399.4 238.9 128.2 88.62 71.00 62.16 71.03 91.22 68.14 68.51 71.04 70.32 78.73 48.84 77.66 586.1 9999.9 3486 42.25 23.25 15.80 11.15 7.923 6.665 5.265 4.232 4.255 4.188 3.961 390.0 8943 715.4 404.7 210.8 123.2 82.98 66.96 63.70 68.87 71.58 60.38 62.68 65.69 60.35 63.41 60.80 52.70 80.39 590.7 9999.9 3702 43.84 21.72 14.37 10.72 7.622 5.948 4.744 4.549 4.593 4.470 400.0 9999.9 722.4 358.5 191.2 119.5 84.63 59.81 60.00 62.63 62.60 55.49 58.89 60.18 56.21 52.73 65.42 53.49 52.06 83.25 585.1 9999.9 3757 41.10 21.45 14.20 9.447 7.064 5.872 5.119 4.312 4.208 410.0 2868 9999.9 361.8 194.8 111.3 75.22 59.91 59.71 60.23 56.83 50.95 53.35 51.04 48.51 46.23 46.41 62.96 43.15 47.38 73.62 554.9 9999.9 3892 38.84 19.25 12.69 8.473 7.011 5.478 4.687 4.833 420.0 1037 9999.9 366.2 166.0 95.67 67.18 57.03 56.77 57.83 51.65 47.63 47.43 46.02 43.75 41.69 41.25 42.98 53.71 39.63 40.86 58.40 544.3 9999.9 3853 37.55 18.75 12.22 8.044 6.376 5.328 5.247 430.0 787.2 4150 9999.9 147.0 91.86 64.65 53.60 52.26 51.84 44.84 44.03 41.59 41.16 38.60 36.13 39.07 36.10 38.37 40.94 31.59 27.62 54.13 535.0 9999.9 3632 36.68 17.04 11.08 8.061 5.963 5.897 440.0 777.9 753.2 9999.9 170.6 94.04 76.67 55.55 51.52 50.32 43.99 38.90 37.19 37.54 36.89 35.71 38.26 35.67 30.09 36.47 29.89 24.15 26.77 53.11 560.2 9999.9 3468 33.86 16.90 11.84 7.832 7.011 450.0 950.2 568.0 5397 9999.9 97.29 76.50 57.36 49.77 47.93 45.37 38.89 34.34 34.93 32.59 35.58 38.88 33.40 27.80 27.20 34.52 23.91 23.23 25.53 53.59 562.4 9999.9 3331 32.84 17.52 12.01 8.504 460.0 838.7 596.1 518.8 9999.9 131.6 80.70 62.38 52.63 47.38 39.34 36.11 35.78 32.45 32.30 33.55 37.29 33.28 26.80 25.15 24.56 30.61 21.28 21.60 24.86 52.35 536.0 9999.9 3500 34.44 17.21 12.52 470.0 849.6 550.4 377.7 5756 9999.9 91.25 66.58 49.17 48.20 39.99 35.26 33.56 30.89 29.24 32.21 37.12 31.97 25.26 23.72 22.69 24.14 26.23 24.84 25.55 25.76 51.95 545.5 9999.9 3962 34.92 20.06 480.0 877.3 530.9 284.3 397.8 9999.9 117.9 69.68 49.92 45.25 43.06 35.19 30.91 29.09 28.62 29.44 34.22 28.79 24.34 22.79 21.90 20.46 23.42 21.25 18.96 18.36 22.46 46.61 505.4 9999.9 4100 36.77 490.0 761.4 552.7 301.4 179.9 5640 9999.9 73.65 48.75 42.40 40.25 33.23 29.32 26.66 26.56 26.89 31.26 25.11 19.60 20.30 18.92 18.38 17.33 22.72 16.41 16.87 16.61 20.01 41.77 494.7 9999.9 4689 500.0 657.7 452.0 277.4 148.3 323.5 9999.9 112.3 56.08 43.77 36.68 31.85 29.65 25.02 24.09 25.38 28.12 22.95 17.03 18.42 18.14 16.48 16.07 16.49 19.41 14.58 13.91 15.85 17.55 41.50 496.3 9999.9 510.0 643.7 381.4 204.5 113.8 108.8 6692 9999.9 60.04 43.35 35.74 30.61 25.99 23.84 22.80 22.15 24.60 20.83 17.12 15.03 15.25 14.57 15.08 13.51 14.37 15.02 12.12 13.53 12.48 16.84 40.93 490.0 520.0 671.9 398.9 226.7 108.5 106.4 356.9 9999.9 105.0 48.45 36.02 29.78 26.58 23.58 22.09 22.33 23.24 18.87 15.27 14.72 12.71 12.90 13.46 13.23 12.40 15.22 12.55 10.69 11.20 12.97 16.86 40.12 530.0 694.0 362.2 215.4 124.5 78.04 102.4 7780 9999.9 59.07 39.16 32.01 25.63 24.07 22.31 21.12 21.22 17.44 13.90 14.05 12.77 11.78 12.28 11.78 11.24 11.95 14.06 9.990 9.844 11.16 12.73 16.36 540.0 598.8 445.6 224.6 121.5 80.19 83.02 387.0 9999.9 114.7 48.14 32.31 28.04 24.58 22.21 21.20 20.92 18.03 13.36 11.55 12.53 11.25 11.42 10.12 11.74 10.91 10.62 12.37 9.255 10.72 11.53 12.27 550.0 611.3 474.2 190.4 103.5 78.59 79.66 84.95 9045 9999.9 58.41 38.04 26.45 24.51 22.22 20.11 20.47 17.01 13.91 12.20 11.47 10.67 10.35 9.789 9.167 10.23 9.238 11.08 9.556 9.233 10.63 11.97 560.0 784.8 324.9 232.2 104.5 79.97 59.01 69.85 429.2 9999.9 103.5 48.79 31.47 26.15 22.41 20.19 20.28 16.31 13.87 13.80 11.18 9.977 10.57 9.290 9.476 8.239 9.747 9.524 11.23 8.853 9.048 10.97 570.0 641.0 435.1 251.7 117.6 63.20 65.92 70.00 85.21 8832 9999.9 63.05 40.60 27.03 23.55 21.20 19.89 16.76 14.54 13.16 12.12 9.698 9.429 8.741 8.807 8.239 7.938 9.094 7.998 10.72 8.642 9.336 580.0 837.4 422.3 232.3 104.1 72.45 60.77 61.44 67.50 421.5 9999.9 116.2 48.27 30.66 23.09 21.84 19.04 17.38 14.86 12.57 14.02 10.43 10.32 9.178 7.056 8.047 7.894 7.756 8.501 9.076 8.998 8.969 590.0 4598 499.3 223.4 135.2 75.46 66.89 51.11 70.96 84.09 9999.9 9999.9 62.75 38.41 27.06 23.10 21.75 17.35 15.62 13.79 13.70 12.31 9.677 8.408 9.047 7.713 7.328 6.910 7.233 7.799 9.840 8.972 600.0 8426 517.4 244.4 133.2 82.28 71.89 56.43 79.30 76.36 473.2 9999.9 112.9 45.11 32.83 24.47 20.64 18.79 16.24 13.71 12.79 18.00 11.23 9.239 8.978 8.335 7.355 7.444 6.331 7.084 8.438 9.616 610.0 4104 529.4 264.3 132.4 77.00 59.63 60.12 72.40 80.49 92.49 9999.9 9999.9 63.50 36.76 28.33 23.91 18.83 17.13 14.87 12.48 11.59 17.73 10.13 9.212 8.051 6.841 7.189 5.939 6.786 7.099 9.228 620.0 1015 4159 278.6 139.8 70.14 56.39 60.61 65.64 86.40 72.29 471.8 9999.9 108.2 48.03 33.16 23.77 21.95 17.39 15.33 13.83 11.96 15.42 11.46 9.470 8.890 8.207 6.661 6.067 5.527 6.314 7.222 630.0 788.7 8897 318.3 129.4 81.62 55.42 59.39 59.04 71.67 72.16 86.76 9999.9 9999.9 61.04 36.83 28.62 22.85 17.78 16.74 15.26 13.01 11.33 24.09 10.43 9.123 7.460 6.895 6.368 6.052 5.649 6.740 640.0 738.2 5331 452.2 136.3 67.68 60.80 52.44 59.01 70.62 86.95 65.18 469.0 9999.9 116.7 47.01 34.10 26.31 20.27 19.18 16.20 14.71 12.65 12.30 21.78 9.514 8.411 7.915 6.186 6.393 6.028 6.703 650.0 753.6 742.3 4071 152.3 79.87 52.71 54.32 63.03 62.00 74.61 58.83 82.54 9999.9 9999.9 60.77 41.42 29.78 25.18 21.78 15.50 15.82 13.58 13.16 19.02 11.54 9.942 9.339 7.415 5.781 6.205 6.644 660.0 952.0 460.6 9999.9 109.8 84.66 57.45 52.05 53.29 59.73 64.24 66.86 60.38 466.9 9999.9 112.3 49.61 34.44 27.41 25.33 21.62 15.66 16.41 15.02 12.65 34.21 10.26 8.481 8.052 6.600 6.763 6.225 670.0 626.5 502.7 6351 383.5 100.5 65.11 65.31 49.35 58.83 58.79 75.25 55.83 83.73 9999.9 9999.9 63.46 43.12 33.47 27.22 22.58 19.86 18.17 17.65 15.58 13.50 28.10 10.59 9.032 8.698 7.783 7.546 680.0 882.4 461.3 650.1 4633 100.5 72.86 74.73 56.88 60.34 73.03 65.41 59.16 70.79 467.8 9999.9 110.7 49.80 36.32 30.16 24.51 24.80 21.59 19.71 17.60 15.34 29.56 14.17 8.810 7.183 8.494 8.409 690.0 578.7 391.1 251.6 9999.9 100.2 90.38 59.25 57.90 54.23 79.15 53.28 76.87 63.11 87.15 9999.9 9999.9 59.66 42.77 35.76 28.40 26.47 24.45 19.33 18.66 14.72 12.87 55.35 9.423 9.058 10.17 8.112 700.0 716.3 342.8 228.0 8022 283.3 74.63 53.06 56.59 58.29 71.85 52.07 70.18 62.77 68.13 475.2 9999.9 110.8 49.14 37.82 29.07 27.29 23.58 20.98 19.52 17.49 15.74 18.42 37.09 9.507 8.219 7.986